50ml Hydrothermal Autoclave Reactor vessel kettle with PTFE Chamber Hydrothermal Synthesis

Hydrothermal Autoclave Reactor vessel kettle with PTFE Chamber Hydrothermal Synthesis 50ml

1.Dati tecnici:

(1) Operating temperature: 220°
(2) Working pressure: 3MPa (gauge)
(3) Heating, cooling rate: 5 c / min
(4) specification 50ml

(5)Size:1 3.8CM*6.3CM(about 5.4*2.5inch)
(20ml, 25ml, 100ml, 150ml, 200ml , 250ml, 300ml, 500ml on sale.)
Packing list：Sold by set

2. Feature:

Il reattore di sintesi idrotermale utilizza acciaio inossidabile di alta qualità. Il corpo del bollitore e il coperchio del bollitore sono sigillati con una struttura di tenuta a cavo durevole e affidabile, l'effetto di tenuta è stabile a lungo termine senza perdite.
Il reattore di sintesi idrotermale con riscaldamento esterno, per ridurre il volume e favorire la reazione nella stessa temperatura di funzionamento del reattore (ad esempio reattore multiplo posto in un forno riscaldato).

3. Methods of operation:

I mezzi di reazione e il corpo del reattore, e per garantire il coefficiente di alimentazione è inferiore a 0,8. Quando il Dipartimento di reazione corrosiva quando si vuole mettere PTFE cespuglio, può essere assicurato solo corpo bollitore dalla corrosione. Il reattore di sintesi idrotermale sarà posto sul riscaldatore, in conformità con le disposizioni del tasso di riscaldamento del riscaldamento alla temperatura di reazione desiderata (inferiore alla temperatura di sicurezza richiesta). Il completamento della reazione avverrà quando il reattore si sarà raffreddato, ma anche in stretta conformità con le disposizioni della velocità di raffreddamento, per facilitare la sicurezza e la durata del reattore. Quando viene confermata una temperatura intra-addominale inferiore al punto di ebollizione dei solventi, il sistema di reazione può aprire il coperchio del serbatoio solo dopo un'operazione di follow-up.
Reattore di sintesi idrotermale da pulire ogni volta dopo l'uso, per evitare la corrosione.
Il corpo del bollitore, la linea di tenuta del coperchio del bollitore devono prestare particolare attenzione alla pulizia e alla prevenzione di danni alle protuberanze.
4.Introduction of “para-polyphenylene (PPL)” lining performance of hydrothermal reactor:
(1) The para-polyphenylene also becomes a polyphenylene, which is a high-linker linked by a benzene ring.
The para-polyphenylene has high temperature resistance and can be used for rocket engine parts and space navigation;
The para-polyphenylene has good thermal stability and can be used to make high temperature bearing materials;
The para-polyphenylene has good corrosion resistance and can be used as a bearing and chemical equipment with corrosive environment and working conditions;
The self-lubricating performance of para-polyphenylene is better than that of molybdenum disulfide and graphite, and can be used to make oil-free lubricating seal rings, packings, piston rings, etc.
Due to the great rigidity and regularity of the molecular chain of the para-polyphenylene, it is infusible and insoluble, and it is difficult to process itself. It needs to be mixed with other materials.
Polyphenylene and polytetrafluoroethylene will be blended to make piston rings, rubber-plastic rails, sealing bushings, fillers, etc., which are used in chemical, light industry, textile, printing and dyeing, machinery and other industries, and achieved good results.
(2) High temperature resistance: The “polyphenylene” powder is burned at 520 °C in the high temperature furnace, and it has no melting point. It is heated at 450 °C for a long time. It is a kind of engineering plastic which is used for a long time below 400 °C. .
(3) Radiation resistance: Under the irradiation of cobalt source (Co60), it can accept 9*106 lats and the performance is unchanged.
(4) Chemical corrosion resistance and solvent resistance type: So far, no solvent has been found in the world for dissolving polyphenylene, and strong acid such as hydrofluoric acid hydrofluoric acid and strong alkali cannot corrode it.
(5) Electrical properties: volume resistivity 1015 ohm-cm, under different polymerization conditions, can become an organic semiconductor, volume resistivity 1017 ohm-cm.
(6) Self-lubricating properties: It has good self-lubricating properties, and is much better than molybdenum disulfide and graphite, or other filled polystyrene-tetrafluoroethylene products.
200ml hydrothermal reactor introduction material:
The kettle body is made of high-quality stainless steel, which is sealed by a circular groove. The manual spiral is strong. It has good sealing performance, high safety factor, low consumption of acid solvent and easy to use!
200ml hydrothermal reactor introduces product features:
1. High temperature resistance: use temperature -200 ~ +300 °C;
2. Low temperature resistance: -196 ° C can be maintained at 5%;
3. Good corrosion resistance, no harmful substances spillage, reduce pollution and safe use.
4. After heating and boosting, the sample which is difficult to dissolve under normal conditions and the sample containing volatile elements can be quickly and non-destructively dissolved.
5. Beautiful appearance, reasonable structure, simple operation, shorten analysis time and reliable data.
6. There are PPL bushings inside to generate care, which can be resistant to acid and alkali.
7. It can replace the platinum ruthenium to solve the problem of sample processing in the analysis of trace elements in high purity alumina. The high-pressure digestion tank used in the oven, also known as a sample dissolver, a pressure-dissolving bomb, a hydrothermal synthesis reactor, and a digester tank, is an environment in which a strong acid or a strong alkali in a tank is used and a high temperature and high pressure is sealed to achieve rapid digestion of poorly soluble substances. purpose. It is a good assistant for digesting samples when measuring trace elements and trace elements. Sample pretreatment to eliminate heavy metals, pesticide residues, food, sludge, rare earths, aquatic products, organic matter, etc.