Chemical lab use reaction tank Customizable lined liner for Hydrothermal Synthesis Autoclave Reactor

High Pressure High Temperature Reactor PTFE Lined Autoclave Hydrothermal Synthetic Digestion Vessels

25mL, 50mL, 100mL, 200mL & 500mL Small Pressure Reactor

A.PTFE lined hydrothermal autoclave (3Mpa, Max.Temperature:220C)

B. PPL lined hydrothermal autoclave (3Mpa, Max. Temperature:280C)

Il reattore di sintesi idrotermale lavora in determinate condizioni di temperatura e pressione per dissolvere il materiale. Il reattore è utilizzato principalmente per materiali che non si dissolvono, per materiali scarsamente solubili o per il prodotto di reazione della sostanza in dissoluzione. Controllando la temperatura della soluzione si ottiene una convezione per formare uno stato supersaturo e la crescita dei cristalli. Il reattore di sintesi idrotermale viene utilizzato per la preparazione o la sintesi di composti di nano materiali. Può anche essere usato per fare piccole reazioni di sintesi della crescita dei cristalli. Il reattore di sintesi idrotermale è ampiamente utilizzato nei laboratori universitari.

Working Temperature：PTFE≤230℃，Safe Temperature is 200℃; PTFE≤280℃，Safe Temperature is 260℃. Strictly require temperature not to exceed the maximum use temperature.
Working Pressure：The pressure of the actual reactant in the kettle shall not exceed 3Mpa. The pressure generated by material synthesis requires the customer to accurately calculate the pressure generated at the temperature according to the different materials used in the experiment. The experiment must be conducted within the normal allowable range to ensure the safety of the experimenter.
PTFE Lining and PPL Lining：PPL is a kind of synthetic material added to PTFE, and its properties are better than those of PTFE alone. PPL can be used continuously at 260 ℃, with the highest operating temperature 280 ℃-300 ℃, very low friction coefficient, good wear resistance and excellent chemical stability.
Loading Capacity：The amount of solvent added to the reaction depends on different tests, generally 60%~80% of the inner cup capacity. If the reactant produces a large amount of gas, it is recommended to cool overnight and use perchloric acid. Hydrogen peroxide and so on should pay special attention!
Heating Equipment and Safety：Generally, the laboratory uses an oven for heating. The actual temperature control inside the oven should reach ± 2 ℃ to avoid excessive overheating. When the oven starts to heat up, there shall be no personnel in the room to prevent explosion injury! Enter the tank only after it is cooled to room temperature. Necessary safety protection measures shall be taken when taking the tank, such as face protection, hand protection, respiratory protection, etc.